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#Post#: 376--------------------------------------------------
Reaction CX-7 (Experimental)
By: Basquyatti Date: September 14, 2018, 1:27 pm
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My experimental synthesis to obtain Halogenated oximes.
Summary: This reaction uses a cheaper process of reducing
Chloropicrin with the help of Magnesium and
anhydrous hydrogen chloride in a closed container, the standard
solvent is Tetrahydrofuran, the reaction takes place at low
temperatures and on vigorous shaking as soon as all the material
is precipitated at the bottom, water is added to precipitate
insoluble, then these are filtered, the solvent distilled and
the CX purified by vacuum distillation.
Using 167.72 grams of PS 99%, place to mix with 600 grams of 99%
THF at 0 degrees Celsius and place the mixture in a
pressure-holding vessel, then introduce 49,102 grams of 99%
Magnesium powder, and close the container with vigorously stir,
pour into it 109.5 grams of anhydrous Hydrogen Chloride, the
reaction ends when there is no more pressure in the vessel, then
it filters the impurities, distills the solvent from 66 degrees
Celsius up to 70 degrees Celsius and distils the agent at 58
degrees Celsius by 28 mmHg
#Post#: 377--------------------------------------------------
Re: Reaction CX-7 (Experimental)
By: zwclose7 Date: September 30, 2018, 11:42 am
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Are you Basquyatti from Wikipedia?
#Post#: 381--------------------------------------------------
Re: Reaction CX-7 (Experimental)
By: Basquyatti Date: October 1, 2018, 11:12 am
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Yes, I am the Basquyati of the Portuguese Wikipedia
#Post#: 382--------------------------------------------------
Re: Reaction CX-7 (Experimental)
By: zwclose7 Date: October 1, 2018, 11:46 am
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Are you a chemist?
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